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TOC Notebook 03

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Michael Huynh edited this page Nov 22, 2011 · 4 revisions

Table of Contents (Notebook 03)

# This is the TOC format:
#   [number] - [description of page]
# For example:
#   005 - Making KBi Solution
# NOTE: The ordering does NOT matter. The entries will be processed and a TOC
#       will be generated with the correct ordering.
  • 001 - Mn-oxide Pourbaix diagram
  • 001 - Mn-oxide mechanistic studies mindmap
  • 001 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8 (AIT1)
  • 001 - CP 3.16e-4A anodization of 32mC Mn-FTO plate in 1M KBi, pH 9.2 (CP2)
  • 002 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8 (AIT3)
  • 002 - CP 1e-3A anodization of 32mC Mn-FTO plate in 1M KBi, pH 9.2 (CP5)
  • 002 - Tafel (CP) 1e-6A to 1e-3A of AIT3's 32mC Mn-FTO in 1M KBi (purest, fresh), pH 9.2 (tafel4)
  • 002 - CP 1e-2A anodization of CP5's 32mC Mn-FTO in 1M KBi, pH 9.2 (CP6)
  • 002 - Tafel (CP) 1e-6A to 1e-3A of CP6's 32mC Mn-FTO in 1M KBi (purest), pH 9.2 (tafel7)
  • 003 - Tafel (CP) plot of 08/26-tafel1 (from NB1): Desorbed 32mC Mn-FTO in 1M KBi (purest, old), pH 9.2
  • 004 - Tafel (CP) plot of 08/29-tafel4 (reproduce p3's tafel): 32mC Mn-FTO, 1M KBi (purest), pH 9.2
  • 004 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8
  • 005 - Tafel (CP) plot of 08/29-tafel7: Stepped anodized 32mC Mn-FTO in 1M KBi (purest), pH 9.2
  • 005 - How much time did I anodize the Mn-FTO plate before in the great 40mV/dec slope plot?
  • 006 - CP 1e-3A anodization of prev AIT's 32mC Mn-FTO for >12hr in 1M KBi (purest, fresh), pH 9.2 (CP1)
  • 006 - Summing charge passed in 08-29-tafel4
  • 006 - Tafel (CP) 1e-6A to 1e-3A of 08/30-CP1's 32mC Mn-FTO in 1M KBi (purest), pH 9.2 (tafel1)
  • 006 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (old), pH 8 (AIT3)
  • 007 - CP 1e-3A anodization of AIT2's 32mC Mn-FTO for >12hr in 1M KBi (purest, fresh), pH 9.2 (CP3)
  • 007 - Making 500mL of 1M KBi (99.99% boric acid and KOH), pH 9.22
  • 008 - Tafel (CP) 1e-6A to 1e-3A of 08/31-CP3's 32mC Mn-FTO in 1M KBi (same, purest), pH 9.2 (tafel1)
  • 008 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (old), pH 8 (AIT3)
  • 008 - CV 0V to 1V of 08/31-tafel1 film in 1M KBi (same, purest), 50mV/s (CV2)
  • 008 - CV 0V to 1.2V of 08/31-tafel1 film in 1M KBi (same, purest), 50mV/s (CV3)
  • 008 - CV 0V to 1.2V of 08/31-tafel1 film in 1M KBi (same, purest), 25 cycles, 100mV/s (CV5)
  • 008 - AIT 0.6V anod on AIT4's Mn-FTO in 1M KBi (purest, fresh), pH 9.2 (AIT6)
  • 009 - Tafel (CP) plot of 08/31-tafel1: high E anodized 32mC Mn-FTO in 1M KBi (pure, fresh), pH 9.2
  • 010 - Preparing 50mL of 0.5M boric acid (purest)
  • 010 - pKa of MnO2 (in Pi)
  • 010 - Tafel (CP) 1e-6A to 1e-3A of 09/01-AIT6's 32mC Mn-FTO in 1M KBi (same, purest), pH 9.2 (tafel1)
  • 010 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (fresh), pH 8 (AIT2)
  • 011 - Tafel (CP) 1e-3A to 1e-6A of AIT2's 32mC Mn-FTO (not anod) in 1M KBi (purest), H->L first, pH 9.2 (tafel3)
  • 011 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (old), pH 8 (AIT4)
  • 011 - Preparing 0.5mM Mn2+, 50mM KBi sol for deposition studies
  • 012 - CV 0.236V to 1.236V of 1cm^2 FTO in Mn-boric acid, pH 4.17, 50 mV/s (CV1)
  • 012 - CV 0.05V to 1.3V of 1cm^2 FTO in Mn-boric acid, pH 4.17, 10 mV/s (CV2)
  • 012 - CV 0.05V to 1.3V of 1cm^2 FTO in Mn-boric acid, pH 4.17, no iR comp, 10 mV/s (CV3)
  • 013 - AIT 0.9V of used FTO in Mn-boric acid, pH 4.17 (AIT5)
  • 013 - AIT 0.9V of AIT4's Mn-FTO in 1M KBi (purest, fresh), pH 9.2 (AIT14)
  • 013 - Bringing pH of Mn-boric acid up to pH 5
  • 014 - CV 0.06V to 1.06V of blank FTO in Mn-KBi, pH 6.98, 50mV/s (CV6)
  • 014 - Again, CV -0.1V to 1.06V of blank FTO in Mn-KBi, pH 6.98, 50mV/s (CV7)
  • 014 - Again, CV 0V to 1.4V of blank FTO in Mn-KBi, pH 6.98, 10mV/s (CV8)
  • 014 - AIT 0.45V for 32mC of CV8's mostly blank FTO in Mn-KBi, pH 6.98 (AIT9)
  • 015 - Tafel (CP) plot of 09/01-tafel1: High E anod of 32mC Mn-FTO in 1M KBi (pure, fresh), pH 9.2
  • 015 - Bringing pH of Mn-KBi solution up to pH 8
  • 016 - Tafel (CP) plot of 09/02-tafel3: No anod of 32mC Mn-FTO, H->L first in 1M KBi (pure, fresh), pH 9.2
  • 016 - CV 0V to 1V of blank FTO in Mn-KBi, pH 7.98, 50mV/s (CV10)
  • 017 - CV -0.1V to 1.2V of blank FTO in Mn-KBi, pH 7.98, 50mV/s (CV11)
  • 017 - Again, CV -0.1V to 1.2V of blank FTO in Mn-KBi, pH 7.98, 10mV/s (CV12)
  • 018 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8 (AIT13)
  • 018 - Tafel (CP) 1e-6A to 1e-3A of AIT14's 32mC Mn-FTO (anod) in 1M KBi (purest), pH 9.2 (tafel15)
  • 018 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (fresh), pH 8 (AIT1)
  • 018 - AIT 0.9V of AIT1's 32mC Mn-FTO in 1M KBi (pure, fresh), pH 9.2 (AIT2)
  • 019 - Preparing fresh 50mL solution of Mn-KBi, pH 9
  • 019 - CV 0.06V to 1.06V blank FTO in Mn-KBi, pH 8.97, 50mV/s (CV3)
  • 019 - Again, CV -0.2V to 1.0V blank FTO in Mn-KBi, pH 8.97, 10mV/s (CV4)
  • 020 - AIT 0.23V for 32mC Mn deposition on blank FTO, pH 8.97 (AIT5)
  • 020 - CV -0.2V to 1.0V blank FTO in Mn-KBi, pH 9.04, 10mV/s (CV1)
  • 020 - Bringing pH of Mn-KBi up to pH 10
  • 020 - CV -0.2V to 0.94V blank FTO in Mn-KBi, pH 10.03, 50mV/s (CV2)
  • 021 - Again, CV -0.2V to 0.94V blank FTO in Mn-KBi, pH 10.03, 10mV/s (CV3)
  • 021 - Thinking about Tafel data
  • 021 - Fe content in boric acid (PURATREM, 99.99% from STREM)
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