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TOC Notebook 03

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Michael Huynh edited this page Jan 30, 2012 · 4 revisions

Table of Contents (Notebook 03)

# This is the TOC format:
#   [number] - [description of page]
# For example:
#   005 - Making KBi Solution
# NOTE: The ordering does NOT matter. The entries will be processed and a TOC
#       will be generated with the correct ordering.

  • 001 - Mn-oxide Pourbaix diagram

  • 001 - Mn-oxide mechanistic studies mindmap

  • 001 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8 (AIT1)

  • 001 - CP 3.16e-4A anodization of 32mC Mn-FTO plate in 1M KBi, pH 9.2 (CP2)

  • 002 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8 (AIT3)

  • 002 - CP 1e-3A anodization of 32mC Mn-FTO plate in 1M KBi, pH 9.2 (CP5)

  • 002 - Tafel (CP) 1e-6A to 1e-3A of AIT3's 32mC Mn-FTO in 1M KBi (purest, fresh), pH 9.2 (tafel4)

  • 002 - CP 1e-2A anodization of CP5's 32mC Mn-FTO in 1M KBi, pH 9.2 (CP6)

  • 002 - Tafel (CP) 1e-6A to 1e-3A of CP6's 32mC Mn-FTO in 1M KBi (purest), pH 9.2 (tafel7)

  • 003 - Tafel (CP) plot of 08/26-tafel1 (from NB1): Desorbed 32mC Mn-FTO in 1M KBi (purest, old), pH 9.2

  • 004 - Tafel (CP) plot of 08/29-tafel4 (reproduce p3's tafel): 32mC Mn-FTO, 1M KBi (purest), pH 9.2

  • 004 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8

  • 005 - Tafel (CP) plot of 08/29-tafel7: Stepped anodized 32mC Mn-FTO in 1M KBi (purest), pH 9.2

  • 005 - How much time did I anodize the Mn-FTO plate before in the great 40mV/dec slope plot?

  • 006 - CP 1e-3A anodization of prev AIT's 32mC Mn-FTO for >12hr in 1M KBi (purest, fresh), pH 9.2 (CP1)

  • 006 - Summing charge passed in 08-29-tafel4

  • 006 - Tafel (CP) 1e-6A to 1e-3A of 08/30-CP1's 32mC Mn-FTO in 1M KBi (purest), pH 9.2 (tafel1)

  • 006 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (old), pH 8 (AIT3)

  • 007 - CP 1e-3A anodization of AIT2's 32mC Mn-FTO for >12hr in 1M KBi (purest, fresh), pH 9.2 (CP3)

  • 007 - Making 500mL of 1M KBi (99.99% boric acid and KOH), pH 9.22

  • 008 - Tafel (CP) 1e-6A to 1e-3A of 08/31-CP3's 32mC Mn-FTO in 1M KBi (same, purest), pH 9.2 (tafel1)

  • 008 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (old), pH 8 (AIT3)

  • 008 - CV 0V to 1V of 08/31-tafel1 film in 1M KBi (same, purest), 50mV/s (CV2)

  • 008 - CV 0V to 1.2V of 08/31-tafel1 film in 1M KBi (same, purest), 50mV/s (CV3)

  • 008 - CV 0V to 1.2V of 08/31-tafel1 film in 1M KBi (same, purest), 25 cycles, 100mV/s (CV5)

  • 008 - AIT 0.6V anod on AIT4's Mn-FTO in 1M KBi (purest, fresh), pH 9.2 (AIT6)

  • 009 - Tafel (CP) plot of 08/31-tafel1: high E anodized 32mC Mn-FTO in 1M KBi (pure, fresh), pH 9.2

  • 010 - Preparing 50mL of 0.5M boric acid (purest)

  • 010 - pKa of MnO2 (in Pi)

  • 010 - Tafel (CP) 1e-6A to 1e-3A of 09/01-AIT6's 32mC Mn-FTO in 1M KBi (same, purest), pH 9.2 (tafel1)

  • 010 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (fresh), pH 8 (AIT2)

  • 011 - Tafel (CP) 1e-3A to 1e-6A of AIT2's 32mC Mn-FTO (not anod) in 1M KBi (purest), H->L first, pH 9.2 (tafel3)

  • 011 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (old), pH 8 (AIT4)

  • 011 - Preparing 0.5mM Mn2+, 50mM KBi sol for deposition studies

  • 012 - CV 0.236V to 1.236V of 1cm^2 FTO in Mn-boric acid, pH 4.17, 50 mV/s (CV1)

  • 012 - CV 0.05V to 1.3V of 1cm^2 FTO in Mn-boric acid, pH 4.17, 10 mV/s (CV2)

  • 012 - CV 0.05V to 1.3V of 1cm^2 FTO in Mn-boric acid, pH 4.17, no iR comp, 10 mV/s (CV3)

  • 013 - AIT 0.9V of used FTO in Mn-boric acid, pH 4.17 (AIT5)

  • 013 - AIT 0.9V of AIT4's Mn-FTO in 1M KBi (purest, fresh), pH 9.2 (AIT14)

  • 013 - Bringing pH of Mn-boric acid up to pH 5

  • 014 - CV 0.06V to 1.06V of blank FTO in Mn-KBi, pH 6.98, 50mV/s (CV6)

  • 014 - Again, CV -0.1V to 1.06V of blank FTO in Mn-KBi, pH 6.98, 50mV/s (CV7)

  • 014 - Again, CV 0V to 1.4V of blank FTO in Mn-KBi, pH 6.98, 10mV/s (CV8)

  • 014 - AIT 0.45V for 32mC of CV8's mostly blank FTO in Mn-KBi, pH 6.98 (AIT9)

  • 015 - Tafel (CP) plot of 09/01-tafel1: High E anod of 32mC Mn-FTO in 1M KBi (pure, fresh), pH 9.2

  • 015 - Bringing pH of Mn-KBi solution up to pH 8

  • 016 - Tafel (CP) plot of 09/02-tafel3: No anod of 32mC Mn-FTO, H->L first in 1M KBi (pure, fresh), pH 9.2

  • 016 - CV 0V to 1V of blank FTO in Mn-KBi, pH 7.98, 50mV/s (CV10)

  • 017 - CV -0.1V to 1.2V of blank FTO in Mn-KBi, pH 7.98, 50mV/s (CV11)

  • 017 - Again, CV -0.1V to 1.2V of blank FTO in Mn-KBi, pH 7.98, 10mV/s (CV12)

  • 018 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi, pH 8 (AIT13)

  • 018 - Tafel (CP) 1e-6A to 1e-3A of AIT14's 32mC Mn-FTO (anod) in 1M KBi (purest), pH 9.2 (tafel15)

  • 018 - AIT 0.38V for 32mC Mn deposition, 1cm^2 FTO in Mn-KMePi (fresh), pH 8 (AIT1)

  • 018 - AIT 0.9V of AIT1's 32mC Mn-FTO in 1M KBi (pure, fresh), pH 9.2 (AIT2)

  • 019 - Preparing fresh 50mL solution of Mn-KBi, pH 9

  • 019 - CV 0.06V to 1.06V blank FTO in Mn-KBi, pH 8.97, 50mV/s (CV3)

  • 019 - Again, CV -0.2V to 1.0V blank FTO in Mn-KBi, pH 8.97, 10mV/s (CV4)

  • 020 - AIT 0.23V for 32mC Mn deposition on blank FTO, pH 8.97 (AIT5)

  • 020 - CV -0.2V to 1.0V blank FTO in Mn-KBi, pH 9.04, 10mV/s (CV1)

  • 020 - Bringing pH of Mn-KBi up to pH 10

  • 020 - CV -0.2V to 0.94V blank FTO in Mn-KBi, pH 10.03, 50mV/s (CV2)

  • 021 - Again, CV -0.2V to 0.94V blank FTO in Mn-KBi, pH 10.03, 10mV/s (CV3)

  • 021 - Thinking about Tafel data

  • 021 - Fe content in boric acid (PURATREM, 99.99% from STREM)

  • 022 - Tafel (CP) plot of 09/02-tafel1: 0.6 V anod of Mn-FTO in 1 M KBi (pure, fresh)

  • 023 - Tafel (CP) plot of 09/03-tafel15: 0.9 V anod of Mn-FTO in 1 M KBi (pure, fresh)

  • 024 - Tafel (CP) of 09/05-AIT2's Mn-FTO in same KBi (pure, fresh), pH 9.2 (tafel3)

  • 024 - Tafel (CP) of blank FTO in 1 M KBi (purest, fresh), pH 9.2 (tafel4)

  • 025 - Brief discussion with Kwabena - loading studies, background.

  • 025 - Tafel (CP) plot of 09/05-tafel3: 0.9 V anod Mn-FTO in 1 M KBi (pure, fresh)

  • 026 - Combined CVs of Mn dep in 1 cm^2 FTO in Mn-KBi from pH 4 to 10, 50 mV/s

  • 026 - Combined CVs of Mn dep in 1 cm^2 FTO in Mn-KBi from pH 4 to 10, 10 mV/s

  • 027 - XRD on 09/05-tafel3: 0.9 V 32mC anod Mn-FTO, dried, 1M KBi

  • 028 - Making 500 mL of 1 M KBi (99.99% boric acid and KOH), pH 9.2

  • 028 - Tafel (CP) plot of 09/06-tafel4: blank FTO in 1 M KBi (purest, fresh), pH 9.2

  • 029 - AIT 0.38 V for 32 mC on 1 cm^2 FTO in Mn-KMePi, pH 8

  • 029 - Attempting to dissolve La nitrate

  • 029 - AIT 1.0 V anod of prev AIT's Mn-FTO in 1 M KBi (pure, fresh), pH 9.2

  • 030 - Tafel (CP) of AIT2's 1.0V anod Mn-FTO in same KBi (fresh, pure), pH 9.2

  • 030 - Making Co electrodes for Seth/MIT Museum display (again)

  • 030 - AIT 0.38 V for 32 mC, 1 cm^2 FTO in Mn-KMePi (old), pH 8 (reduplicate)

  • 031 - AIT 1.0 V anod of AIT1's Mn-FTO in 1 M KBi (pure, fresh), pH 9.2 (AIT2)

  • 031 - Tafel (CP) of AIT2's 1.0V anod Mn-FTO in same KBi (fresh, pure), pH 9.2

  • 032 - Group meeting (Dilek) - electrocatalytic H2 evolution with NiHPXBr.

  • 032 - Tafel (CP) plot of 09/10-tafel3: 1.0 V anod Mn-FTO in KBi (fresh, pure), pH 9.2

  • 032 - Tafel (CP) plot of 09/15-tafel1: 1.0 V anod Mn-FTO in KBi (fresh, pure), pH 9.2

  • 033 - AIT 1.0 V 32 mC dep, 1 cm^2 FTO in Mn-KMePi (old), pH 8 (AIT1)

  • 033 - Tafel (CP) of AIT1's Mn-FTO in 1 M KBi (pure, fresh), pH 9.2 (tafel2)

  • 034 - Solubility of lead phases

  • 034 - Solubility of iron phases

  • 034 - Solubility of lanthanum salts

  • 035 - AIT 0.38 V, 32 mC, 1 cm^2 FTO dep in Mn-KMePi (fresh), pH 8 (AIT2)

  • 035 - Checking of Mn will deposit in various media

  • 035 - CV blank FTO in 0.5 mM Mn, 50 mM KNO3, 0V to 1.3V, 50 mV/s

  • 064 - Making 50 mL of 1 M phosphoric acid

  • 065 - CV 0V to 1.4V of blank FTO in 0.5 mM Mn(2+), 50 mM KPi, pH 3.18, 50 mV/s

  • 066 - CV 0V to 1.4V of blank FTO in 0.5 mM Mn(2+), 100 mM KPi, pH 7.22, 50 mV/s

  • 067 - CV -0.1V to 1.0V of blank FTO in 0.5 mM Mn(2+), 100 mM KPi, pH 8.08, 50 mV/s

  • 067 - CV -0.1V to 1.0V of blank FTO in 0.5 mM Mn(2+), 100 mM KPi, pH 8.08, 10 mV/s

  • 084 - Making 500 mL of 1 M KPi, pH 7.20

  • 086 - Actually making 500 mL of 1 M KPi, pH 7.20

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